From the Japan Society for Analytical Chemistry, Analytical Sciences is a completely free journal covering topics related to "the theory and practice of analytical sciences, including fundamental and applied, inorganic and organic, wet chemical and instrumental methods." Full-text content is available beginning 1998 (Vol 14); Table of Contents begins December, 1992 (Vol 8).
Volumes 6-8 of Trends in Analytical Chemistry are available online for free to members of ChemWeb (no charge, registration required). The special June issue covers Nanoscale chemical analysis. Articles can be downloaded in .pdf format or read as HTML files.